Chemical Food Contaminants Analysis, 1st ed. 2024 Methods and Protocols in Food Science Series

This volume provides protocols on different combinations of contaminates, matrices, and sample preparation. Chapters are divided into two parts, detailing polycyclic aromatic hydrocarbon,dioxins, furans, organochlorie pesticides, toxic elements, mycotoxins, mercury in food products, acrylamine, polypeptide antibiotics, tetracyclines, coccidiostats, beta-blockers, sedatives,glucocorticoids, palytoxin-like marine biotoxins in fish, polar drugs and contaminants in animal feed, UV filters, micro and nanoplastics in seafood, tetracyclines in vegetables, MCPDEs, and pharmaceuticals in seafood. Written in the format of the Methods and Protocols in Food Science (MeFS) series, the chapters include an introduction to the respective topic, list necessary materials and reagents, detail well-established and validated methods for readilyreproducible laboratory protocols, and contain notes on how to avoid or solve typical problems.

 Authoritative and cutting-edge, Chemical Food Contaminants Analysis aims to ensure successful results in the further study of this vital field

Part I

1. Determination of polycyclic aromatic hydrocarbons (PAHs) in seafood by matrix solid-phase dispersion and pressurized liquid extraction followed by GC-MS/MS analysis

Luana de Souza Futigami, Ana Paula Zapelini de Melo, Carolina Turnes Pasini Deolindo, Cristian Rafael Kleemann , Vívian Maria Burin, and Rodrigo Barcellos Hoff  

2. Determination of polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs), and dioxin-like polychlorinated biphenyls (dl-PCBs) in food by GC-MS/MS

Rafael Pissinatti,Matheus M. M. F. Gloria, Rafael F. Mota, Christiane R. Rocha, and Raquel Nogueira

3. Simultaneous analysis of polychlorinated biphenyls (PCBs) and organochlorine pesticides (OCPs) in animal fat by GC-ECD and GC-MS

Cláudia Hoffmann Kowalski Schröder

4. Determination of As, Cd, Hg and Pb in milk, meat, rice, and garlic by ICP-MS

Daiane Cioato and Lucas Suchecki Barnet

5. Determination of sedatives and ����-blockers residues in bovine, swine, and equine kidney by liquid chromatography coupled to tandem mass spectrometry

Lenise Guimarães de Oliveira, Fabiano Barreto, Carolina Turnes Pasini Deolindo, Cristian Rafael Kleemann, Luciano Molognoni, Rodrigo Barcellos Hoff, and Fábio Ferreira Gonçalves

6. Determination of pesticides and mycotoxins in malt, brewers’ spent grain, and beer using a dilute-and-shoot procedure and HPLC-MS/MS

Nilsrael Alves Pires, Mauro Lucio Gonçalves De Oliveira, José Ailton Gonçalves, and Adriana Ferreira Faria

7. Screening of antimicrobials residues in muscle from different species by liquid chromatography coupled with tandem mass spectrometry

8. Determination of ochratoxin A in plant products: immunoaffinity column and liquid chromatography with fluorescence detector

9. Total mercury determination in fish muscle: direct analysis by atomic absorption spectrophotometer

10. Determination of polypeptide antibiotics in milk by simple LLE technique and LC–MS/MS analysis

Mauricio Perin

11. Determination of tetracyclines and their 4-epimers in milk by solid-phase extraction (SPE) and liquid chromatography tandem mass spectrometry

Rosana Gomes Ferreira, Mararlene Ulberg Pereira, Amanda da Silva Rio, and Bernardete Ferraz Spisso

Renata de Faria Barbosa, Chariston Andre Dal Belo, Carla da Silva Carneiro, and  Eliane Teixeira Mársico

13. Determination of acrylamide in sweet potato products using QuEChERS sample preparation followed by LC-ESI-MS/MS analysis

Cristiane Lopes Pinto Ferreira, Patricia Aparecida de Campos Braga, and Adriana Pavesi Arisseto Bragotto

14. Determination of p-nitroaniline residues in chicken meat by salting-out liquid-liquid extraction (SALLE) followed by derivatization and LC-MS/MS analysis

Vivian Feddern, Vanessa Gressler, Anildo Cunha Jr., and Danniele Miranda Bacila

15. Determination of glucocorticoid residues in bovine, swine, and equine liver by liquid chromatography coupled to tandem mass spectrometry

Fabiano Barreto, Carolina Turnes Pasini Deolindo, Cristian Rafael Kleemann, and Rodrigo Barcellos Hoff

Part II:

16. Screening of contaminants of emerging concern (CECs) in fish and milk samples by liquid chromatography coupled with high-resolution tandem mass spectrometry (LC-HRMS/MS)

17. Determination of N-nitro-, C-nitro-, and C-nitrous-type compounds in meat products by d-SPE extraction and liquid chromatography coupled to mass spectrometry

Luciano Molognoni , Heitor Daguer, and Rodrigo B. Hoff

18. Determination of polar veterinary drugs and melamine in feeds: method using  ion-pair reversed-phase or hydrophilic interaction liquid chromatography coupled to tandem mass spectrometry

Luciano Molognoni, Ana Paula Zapelini de Melo, Thais de Oliveira, and Cristian Rafael Kleemann

19. Miniaturized extraction method based on bead beating tissuelyser for the analysis of pharmaceuticals in seafood

Lúcia H.M.L.M. Santosand Sara Rodríguez-Mozaz

20. Determination of UV filters and metabolites in seafood by HPLC-MS/MS

M. Silvia Diaz-Cruz and Gemma Vilaró

21. Determination of palytoxins oxidation products in seafood using solid phase extraction and liquid chromatography-tandem mass spectrometry

Cristian Rafael Kleemann, Milena Dutra Pierezan, Pedro Luiz Manique Barreto, Silvani Verruck, and Rodrigo Barcellos Hoff

22. A rapid method for screening microplastic in seafood using Nile Red (NR) and fluorescence preceding spectroscopic polymer analysis

Mariana Gonzalez, María Soledad Islas, Francesca Maria Mitton, and  Mauricio Díaz-Jaramillo

23. Determination of pyrrolizidine alkaloids in plants, pollen, and honey by LC-ESI-MS/MS

Ana Carolina Oliveira Costa, Andressa Camargo Valese, Luciano Molognoni, Heitor Daguer, Bibiana da Silva, and Patricia Brugnerotto

24. Conventional and dispersive solid phase extraction clean-up approaches for the simultaneous analysis of tetracyclines and sulfonamides in a variety of fresh vegetables

I. Vergara-Luis, J.C. Báez-Millán, I. Baciero, B. González-Gaya, M. Olivares, O. Zuloaga, and  A. Prieto

25. Determination of 2-monochloropropane-1,3-diol esters (2-MCPDE), 3-monochloropropane-1,2-diol esters (3-MCPDE) and glycidyl esters (GE) in marine oil-based supplement by acid transesterification via gas chromatography coupled to mass spectrometry (GC-MS)

Ana Paula Ferreira de Oliveira, Fernanda Moralez Leme Gomes, Eduardo Vicente, and Adriana Pavesi Arisseto Bragotto

Includes cutting-edge methods and protocols

Provides step-by-step detail essential for reproducible results

Contains key notes and implementation advice from the experts